COMPARATIVE STUDY OF TWO CLASSICAL EXTRACTION METHODS BY USING GC/MS OF TEPHROSIA NUBICA BOISS GROWING IN SAUDI ARABIA
Journal Title: European Journal of Pharmaceutical and Medical Research - Year 2018, Vol 5, Issue 3
Abstract
A comparative study was done at first time from the aerial parts of T. nubica Boiss growing in S. A. by using two conventional extraction techniques Macerated (MA) & Soxhlet (SX) and analyzed by GC & GC/MS. In this work, we compare the extraction effectiveness of two methods commonly applied in lab. Also, a comparison of extracting solvents was performed in current study. The extraction conditions might not be maximized for these two techniques; the select of extraction parameters were depend on the experience from pervious investigation published worldwide. This study focused on the vast variation of the extraction quantities and quality with MA & SX methods. The GC & GC/MS chromatographic analysis results found have observed that the alcohol can give the highest recoveries when compared to other extraction solvents. The comparison made between the MA and SX extraction methods has found that MA is a suitable alternative to SE for the hexane and chloroform chemical composition, but SX did not give a good recovery by these two solvents. This study is the first report describing comparison between MA and SX by using GC & GC/MS.
Authors and Affiliations
Dr. Hanan Al-Yousef
Keywords
Related Articles
- EP ID EP635385
- DOI -
- Views 114
- Downloads 0
A REVIEW ON THIRD GENERATION CEPHALOSPORINS
Rational use of drugs refers as patients receive medicines according to their clinical needs at lowest cost. The beta lactam antibiotics alter cell wall biosynthesis. Cephalosporins belong to beta lactam antibiotics and...
RETROSPECTIVE STUDY OF THE PREVALENCE AND PATTERN OF PARVOVIRAL ENTERITIS PRESENTED AT THE VETERINARY TEACHING HOSPITAL, UNIVERSITY OF IBADAN, NIGERIA.
Canine Parvovirus Enteritis remains a significant cause of mortality and morbidity in dogs in Nigeria. To assess its prevalence and pattern of occurrence, case records of dogs presented with gastroenteritis at the Veteri...
ANALYSIS FOR EPHEDRINE ALKALOID UTILIZING ISOCRATIC HIGH PERFORMANCE LIQUID CHROMATOGRAPHY
A method to assay ephedrine hemihydrate (ephedrine alkaloid), which has various biological activities, is presented using isocratic high performance liquid chromatography (HPLC). Elution of the analyte is detected with u...
THE BIO TOXICITY OF IN-SITU SYNTHESIZED CARBOXYLATED NANODIAMOND-IRON OXIDE NANOCOMPOSITE
Nanodiamond (ND) particles have potential applications in protein immobilization, biosensors, therapeutic molecule delivery and bio imaging. A nanocomposite comprises both high hardness of nanodiamond (ND) and high magne...
YELLOW FEVER VIRUS (YFV) INFECTION EVALUATION USING RAPID DIAGNOSTIC TESTS (RDTS) BASED ON ANTI-YFV IGM/IGG
Yellow fever (YF) is an acute viral haemorrhagic disease transmitted by infected genus Aedes mosquitoes. The yellow fever virus (YFV) is mostly found in tropical and subtropical areas of Africa and South America. Outbrea...