Microwave-assisted multicomponent reaction for the synthesis of 2-amino-4H-chromene derivatives using ilmenite (FeTiO3) as a magnetic catalyst under solvent-free conditions

Journal Title: Asian Journal of Green Chemistry - Year 2017, Vol 1, Issue 1

Abstract

A green and highly efficient method has been developed for the synthesis of 2-amino-4H-chromene derivatives in the presence of FeTiO3 as magnetic catalyst via one-pot three-component condensation reaction of aromatic aldehydes, malononitrile and α- or β-naphthol without solvent under microwave irradiation. Mild reaction conditions, short reaction times, simple work-up, use of an economically convenient catalyst, and excellent product yields are the advantageous features of this method. The catalyst can be easily recovered by a simple magnetic separation and can be recycled six times with no significant loss of catalytic activity.

Authors and Affiliations

Ali Ramazani, Saeid Taghavi Fardood, Behrooz Ebadzadeh, Pegah Azimzadeh Asiabi, Yousef Bigdeli Fard

Keywords

Related Articles

Green synthesis and antibacterial activity of cadmium sulfide nanoparticles (CdSNPs) using Panicum sarmentosum

The plant sources can act as potential precursors for the synthesis of nanoparticles in non-hazardous ways as plants contain various secondary metabolites, acting as reducing and stabilizing agents for the reduction reac...

Facile ionic liquid-mediated, multi component synthesis of dihydro-1H-furo[2,3-c]pyrazoles

A facile, convenient, efficient, and high-yielding diastereoselective synthesis of a novel fused dihydro-1H-furo[2,3-c]pyrazole by a one-pot four-component reaction of β-keto ester, hydrazine, aromatic aldehyde and pyrid...

A review on plant extract mediated biogenic synthesis of CdO nanoparticles and their recent applications

Development of an environmentally benign route for synthesis of nanomaterial is a remarkable step in the field of nanotechnology. Nanotechnology involves the tailoring of materials at the atomic level to attain peculiar...

Bio fabricated of silver nanoparticles using Ocimum basilicum and its efficacy of antimicrobial and antioxidant activity

To resolve the efficacies of antibacterial, antifungal, and antioxidant activities of aqueous leaf extract of Ocimum basilicum mediated biosynthesis of silver nanoparticles (Ag-NPs). Aqueous and synthesized Ag-NPs were t...

Synthesis of spiro [cyclobutane-1,2'-indene]-1',3'-dione under a new multi-site phase-transfer catalyst combined with ultrasonication-a kinetic study

In the present study, kinetics of synthesis of spiro[cyclobutane-1,2’-indene]-1’,3’-dione was successfully carried out by spirolation of indene-1,3-dione with 1,3-dibromo propane using aqueous potassium hydroxide and cat...

Download PDF file
  • EP ID EP252339
  • DOI 10.22631/ajgc.2017.93142.1006
  • Views 123
  • Downloads 0

How To Cite

Ali Ramazani, Saeid Taghavi Fardood, Behrooz Ebadzadeh, Pegah Azimzadeh Asiabi, Yousef Bigdeli Fard (2017). Microwave-assisted multicomponent reaction for the synthesis of 2-amino-4H-chromene derivatives using ilmenite (FeTiO3) as a magnetic catalyst under solvent-free conditions. Asian Journal of Green Chemistry, 1(1), 34-40. https://europub.co.uk/articles/-A-252339