NMR Assignment of N-(1-adamantyl)-1-pentyl-1H-indazole-3-carboxamide Seized as Herbal Incense for the First Time in Italy
Journal Title: Journal of Forensic Science & Criminology - Year 2014, Vol 2, Issue 1
Abstract
The synthetic cannabinoid, N-(1-adamantyl)-1-pentyl-1H-indazole-3-carboxamide, known also as AKB48 and/or APINACA, has been detected for the first time in herbal incense seized in Italy. Its structural characterization has been performed through gas chromatography-mass spectrometry (GC-MS) and high-resolution nuclear magnetic resonance (NMR) analysis. In order to favor an easier and faster identification of AKB48 in future investigations, NMR assignments in deuterated methanol and chloroform is also reported.
Authors and Affiliations
Antonio Randazzo
Legal Medical Age Estimation in Portuguese Adult Cadavers: Evaluation of the Accuracy of Forensic Dental Invasive and Non-Invasive Methods
Age estimation of unknown human cadavers is important in setting a crime investigation, such as homicide, suicide or in mass disaster because it can guide forensic investigators to the correct identity among a large numb...
The Forensic Science Effect
As a criminal defense attorney and criminology professor, I am amazed and excited that so many Americans have an interest in forensic science. When striking juries, I used to ask how many jurors watched television shows...
Law & Psychiatry in India: An Overview
The application of legal knowledge to psychiatry and of psychiatric knowledge to the legal issues is the subspecialty of psychiatry known as forensic psychiatry. In India, forensic psychiatry is still in its infancy. The...
Tame to Torture: Psychosexual Correlations of Sex, Violence and Torture
This paper discusses the psychosexual correlations and psychological consequences related to torture and behavioral acts that are fundamentally torturous. The influence of participation by learning and the relationship o...
The Impact of Advances in Post-Mortem Imaging on Forensic Practice
Post-mortem imaging in the form of plain X-ray films has been in use for many years as an adjunct or occasionally as a substitute for autopsy. However, in the last two decades there has been increasing interest and inves...