Structure and Molecular Interactions Analysis of (E)-N′-(3,4,5-trimethoxybenzylidene) isonicotinohydrazide dihydrate
Journal Title: IOSR Journal of Applied Physics (IOSR-JAP) - Year 2018, Vol 10, Issue 6
Abstract
The compound (E)-N′-(3,4,5-trimethoxybenzylidene)isonicotinohydrazide dihydrate crystallizes in the monoclinic space group P21/n with unit cell parameters a = 9.1136(9) Å, b = 16.3007(13) Å, c = 11.7446(10) Å, β = 91.425(9)º and number of molecules per unit cell (Z) = 4. The crystal structure was solved by direct methods and refined by full matrix least squares procedures to a final R value of 0.070 for 1809 observed reflections. The Schiff base molecule exists in E conformation with respect to the C=N double bond. The structure exhibits inter-molecular H-bonds of the type O-H…N, O-H…O, N-H…O and C-H…O.
Authors and Affiliations
Gopal Sharma, Sumati Anthal, A. Jayashree, B. Narayana, B. K. Sarojini, Rajni Kant
Keywords
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- EP ID EP443071
- DOI 10.9790/4861-1006023944.
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