Synthesis and Characterization of Bis-Acetylacetonatozink (II) [(Zn(acac)2(H2o)]
Journal Title: International Journal of Current Science Research and Review - Year 2024, Vol 7, Issue 06
Abstract
The synthesis of the bis-acetylacetonate zink (II) monohydrate complex [Zn(acac)2(H2O)] has been conducted. FTIR analysis, TGA-DSC, and SEM micrographic analysis performed complex characterization. The yield of the complex compound [Zn(acac)2(H2O)] was 36.24% using NaOH as a pH regulator. Based on the FTIR characterization of the typical absorption complex [Zn(acac)2(H2O)] appears at 763.88 cm-1 for Zn-O, C-H at 933.9 cm-1 and 1020 cm-1, C=C and C=O at 1516 cm-1, 1610 cm-1 and OH at 3450 cm-1 respectively. Thermal analysis of the complex shows that the decomposition temperature was obtained at 186oC. Based on the micrographic results, the complex has a non-uniform surface relief. The complex has an even distribution of pores with non-uniform pore sizes. Zn particles are deposited on the complex surface with various sizes to produce pores on the solid surface.
Authors and Affiliations
Laode A. Kadir, Thamrin Azis, Imran . , La Ode Kadidae, Ida Usman, Agusriyadin .
Keywords
Related Articles
- EP ID EP738961
- DOI 10.47191/ijcsrr/V7-i6-83
- Views 44
- Downloads 0
Efficacy of Some Plant Extracts Against Stored-Product Pest Red Flour Beetle, Tribolium Confusum (Jacquelin Du Val) (Coleoptera: Tenebrionidae) Adults
The efficacy of five plant extracts, Lantana camara, Ruta chalepensis, Rhazya stricta, Heliotropium bacciferum and Marrubium vulgare against Tribolium confusum ware investigated by admixing plant extract with wheat grain...
Development of OLMP Model Teaching Modules on SPLTV Material to Improve Students' Creative Thinking Skills
Learning in the classroom that does not utilize media optimally causes the class to be boring, inhibits independence, and limits students from seeking knowledge. Apart from that, students’ creative thinking abilities in...
Assessment of Physico-chemical Parameters of water quality of Ground Water, Almanagil town, Gezira State, Sudan
The current study was conducted to evaluate physical and chemical parameters of water quality taken from some of ground wells in Almanagil town, Gezira State, Sudan. The efforts, in this work, included a collection of...
Adaptation Factor Analysis Instrument of Interpersonal Support Evaluation List in Indonesian Version: Confirmatory Approach
Social support is an interpersonal transaction that involves one or more things such as emotional attention, instrumental assistance, information, and appraisal. Social support comes from the perception that there are pe...
A Case of Candida-Associated Intestinal Perforation in a 16-Month Old Child: A Rare Complication of Gastroenteritis with Fatal Outcome
Introduction: Acute gastroenteritis (AGE) remains a leading cause of childhood morbidity and mortality worldwide, predominantly caused by viral, bacterial, or protozoal infections. However, rarely, AGE can be caused by f...