Synthesis and Characterization of Bis-Acetylacetonatozink (II) [(Zn(acac)2(H2o)]
Journal Title: International Journal of Current Science Research and Review - Year 2024, Vol 7, Issue 06
Abstract
The synthesis of the bis-acetylacetonate zink (II) monohydrate complex [Zn(acac)2(H2O)] has been conducted. FTIR analysis, TGA-DSC, and SEM micrographic analysis performed complex characterization. The yield of the complex compound [Zn(acac)2(H2O)] was 36.24% using NaOH as a pH regulator. Based on the FTIR characterization of the typical absorption complex [Zn(acac)2(H2O)] appears at 763.88 cm-1 for Zn-O, C-H at 933.9 cm-1 and 1020 cm-1, C=C and C=O at 1516 cm-1, 1610 cm-1 and OH at 3450 cm-1 respectively. Thermal analysis of the complex shows that the decomposition temperature was obtained at 186oC. Based on the micrographic results, the complex has a non-uniform surface relief. The complex has an even distribution of pores with non-uniform pore sizes. Zn particles are deposited on the complex surface with various sizes to produce pores on the solid surface.
Authors and Affiliations
Laode A. Kadir, Thamrin Azis, Imran . , La Ode Kadidae, Ida Usman, Agusriyadin .
Re-actualization of Traditional Themes in Contemporary Craft Art through the Concept of Hybrid Aesthetics
In the beginning, craft as a category of art was established because of its traditional cultural elements. However, in its development, contemporary craft art features many other styles and elements of art, making it dif...
Relevance of IPR in Small Businesses
Small businesses in India have always been one of the major occupations in rural as well as urban terrain and they are major source of income for the middle class group. As urbanization has increased the demand for the s...
Challenges and Strategies in the Return of Land Bailout Funds for Toll Road Construction: A Detailed Analysis of PT Hutama Karya's Approach
This study explores the factors that cause the delay in the process of returning the Land Bailout Fund (LBF) and examines potential problems related to the inability of the Government of Indonesia to return LBF to PT Hut...
The Results of Vaccination and Reversed After Vaccination of Coronavirus Infection in Fergana Region for 2021–2022
In this study, an analysis of the incidence of COVID–19 in the Fergana region was carried out, the number of vaccinated vaccination coverage and those who recovered after vaccination with COVID–19 was determined. The inc...
The Influence of Good Corporate Governance on Firm Value before and during COVID-19 in Indonesia
This study investigates the impact of independent commissioners, audit committees, institutional ownership, and managerial ownership on the firm value of Indonesian manufacturing companies, both before and during the COV...