Synthesis and characterization of calcium ferrite nanoparticles by solution combustion method
Journal Title: Bulletin of Pure and Applied Sciences Sec. C – Chemistry - Year 2018, Vol 37, Issue 1
Abstract
The current paper has focussed on the synthesis and characterization of calcium ferrite nanoparticles by solution combustion method. Calcium ferrite nanoparticles were prepared by a solution based method using calcium chloride (CaCl2), ferrous sulphate (FeSO4), dl–Alanine and sodium hydroxide (NaOH) as a precipitant and the obtained precipitation was calcined under 500 C for 4 hours. The resulting material was characterized by using X–ray diffractometry, Scanning electron microscopy, FTIR Spectroscopy and UV–Vis spectroscopy. The magnetic characterization was done by using a vibrating sample magnetometer. The electrical conductance, salinity and total dissolved solid measurements of the prepared nanoparticles were conducted. From PXRD results the calculated crystalline size is 12 nm. SEM micrograph reveals the formation of spherical structures. The FTIR spectrum confirms the Ca–O and Fe–O bonds in the sample. The VSM analysis reveals that the particle shows superparamagnetism.
Authors and Affiliations
Vidya VG
Keywords
Related Articles
- EP ID EP526503
- DOI 10.5958/2320-320X.2018.00018.3
- Views 135
- Downloads 0
Structural, Bonding and Spectral Analysis of an anti-malarial drug 5-(4-chloro phenyl)-6-ethyl-2,4-pyrimidinediamine
Antimalarial drug 5–(4–chlorophenyl)–6–ethyl–2,4–pyrimidinediamine (PYR) was investigated using FT IR and FT Raman spectra along with its molecular geometry, natural bond orbital and its molecular electrostatic potential...
Synthesis of 1,2,3–benzotriazol–1–yl–[n–(n’–arylthiocarbamoyl)] amidines
Synthesis of hitherto unreported 1,2,3–benzotriazol–1–yl–[N–(N’–arylthiocarbamoyl)] amidines from benzo–1,2,3–triazol–1–ylamidinium p–toluene sulfonate is reported
Synthesis and Characterization of Polymer Metal Complexes of Cu (II) and Zn (II) with NNMBA Cross-Linked Polyacrylamide Supported L-Aspartic Acid and L-Lysine
Crosslinked polymers with specific properties are widely used as catalyst supports as they are inert, non toxic and non volatile and offer advantageous features of heterogeneous catalysis such as thermal stability, selec...
Excess Molar Enthalpies of Acetylene Tetrachloride with Furan, Methylfuran, Tetrahydrofuran and 1,4-dioxane at the Temperature 308.15K
The excess molar enthalpies HE of mixtures of acetylene tetrachloride with furan or methylfuran or tetrahydrofuran or 1,4-dioxane have been measured over the entire composition range at the temperature Ts 308.15 K. Th...
Solid state synthesis of 5–anilino–3–(3,5–dimethylpyrazol–1–yl)–1,2,4–thiadiazoles
We wish to report the synthesis of 5–anilino–3–(3,5–dimethylpyrazol–1–yl)–1,2,4–thiadiazoles by a solid state, mechanochemical oxidative cyclization of 3,5–dimethyl–1–[N–(N’–arylthiocarbamoyl) amidino] pyrazoles, which...