Synthesis, Crystal Structure and Characterization of Cu2 (PO4) (OH)
Journal Title: JOURNAL OF ADVANCES IN CHEMISTRY - Year 2013, Vol 5, Issue 2
Abstract
This paper reports the hydrothermal synthesis and crystal structure refinement of cuivre phosphate hydroxide,  Cu 2 (PO4) (OH), obtained at 453 K.Its structure consists of chains of edge-sharing, distorted [CuO4 (OH)2] octahedral extending parallel to [001]. These chains are cross linked by isolated PO4 tetrahedra through corner-sharing, forming channels in which dimmers of edge-sharing [CuO4 (OH)] trigonal bipyramids are located. The structure is stabilized by medium to weak O-H…O hydrogen bonds. In contrast to the previous refinement single crystal X-ray and analysis of data from vibrational spectroscopy, all non –H atoms were refined with anisotropic displacement parameters and the H atom was located.
Authors and Affiliations
R. Ayadi, Mohamed Boujelbene, T. Mhiri
Keywords
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- EP ID EP652585
- DOI 10.24297/jac.v5i2.2658
- Views 181
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