Synthesis, Growth and Characterization of N-(3-Nitrophenyl) Acetamide Crystal- Find it Optical Uses
Journal Title: International Journal of Engineering Sciences & Research Technology - Year 30, Vol 2, Issue 10
Abstract
Single crystals of N-(3-nitrophenyl)acetamide (3-NPA) were successfully grown by slow evaporation method at a constant temperature 32°C from acetone and methanol mixed solvent. The suitability of the selected mixed solvent was justified by the growth of large size, transparent single crystal of 3-NPA. The solubility studies for 3-NPA were estimated. The cell dimensions were obtained by powder crystal X-ray diffraction (XRD) study. The functional groups have been confirmed using Fourier transform infrared (FTIR) analysis. UV-visible and fluorescence spectral analyses were carried out for the grown crystals. Thermo gravimetric analysis and differential thermal investigation were carried out to find out the thermal properties of the as grown crystal. The Second Harmonic Generation (SHG) efficiency of 3-NPA was also determined using Kurtz-Perry method.
Authors and Affiliations
S. Vijayakumar
Keywords
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