pH Assist for Highly selective determination of Xipamide by the enhancement of the green emission of Tb3+ optical sensor
Journal Title: JOURNAL OF ADVANCES IN CHEMISTRY - Year 2014, Vol 10, Issue 5
Abstract
The highly selective, accurate method for determination of Xipamide was maintained. The method depends on the enhancement of the green emission band of Tb3+ at 545 nm in the presence of different concentration of  Xipamide at pH 4.1 and λex = 320 nm in acetonitrile. The photophysical properties of the green emissive Tb3+ complex have been elucidated, the terbium was used as optical sensor for the assessment of  Xipamide in the pharmaceutical tablets and body fluids with a concentration range 5.0 ×10−9 – 2.3 ×10−6 mol L−1 of xipamide, correlation coefficient of 0.995 and detection limit of 8.5 ×10−10 mol L−1.
Authors and Affiliations
M. S. Attia, A. O. Yuossef, M. Diab, M. F. El-Shahat
Keywords
Related Articles
- EP ID EP652755
- DOI 10.24297/jac.v10i5.889
- Views 174
- Downloads 0
Investigation of Inhibition Effect and Determination of Some Quantum Chemical Parameters of an Organic Compound on the Carbon Steel in Sulfuric Acid Medium
The inhibition ability of [3-(4-methyl-pyridin-2-y1)-4-oxo-2-phenylimino-thiazolidin-5-ylidene]-acetic acid ethyl ester (MOTAE) on the corrosion behavior of carbon steel in 0.5 M sulfuric acid solution was investigated u...
Detection and Classification of Leukemia using MPFCM Segmentation and Random Forest with Boosting Techniques
Identification of blood disorders is through visual inspection of microscopic blood cell images. From the identification of blood disorders lead to classification of certain diseases related to blood. We propose an autom...
Concrete Incorporated With Silica Fume And Manufactured Sand Under Acidic Nature
Now a dayAcid attack is growing threat to concrete structures. Using some alternate materials as partial replacement of cement and sand in the concrete is an important factor that enhances the performance of concrete in...
Experimental Study of Environment Friendly Mixed Refrigerant to Replace R-134a in a VCR System with Testing and Training of ANN
This work presents an experimental study on environment friendly mixed refrigerant to replace R134a in vapour compression refrigeration (VCR) System. The mixed refrigerants investigated are propane (R290), butane (R600),...
Egyptian Propolis Alleviates Gentamicin-Induced Nephrotoxicity in Rats
The objective of this study was to evaluate the effectiveness of oral administration of ethanol extract of propolis against gentamicin induced nephrotoxicity in rats. Oral administration of ethanol extract of propolis (E...