pH Assist for Highly selective determination of Xipamide by the enhancement of the green emission of Tb3+ optical sensor
Journal Title: JOURNAL OF ADVANCES IN CHEMISTRY - Year 2014, Vol 10, Issue 5
Abstract
The highly selective, accurate method for determination of Xipamide was maintained. The method depends on the enhancement of the green emission band of Tb3+ at 545 nm in the presence of different concentration of  Xipamide at pH 4.1 and λex = 320 nm in acetonitrile. The photophysical properties of the green emissive Tb3+ complex have been elucidated, the terbium was used as optical sensor for the assessment of  Xipamide in the pharmaceutical tablets and body fluids with a concentration range 5.0 ×10−9 – 2.3 ×10−6 mol L−1 of xipamide, correlation coefficient of 0.995 and detection limit of 8.5 ×10−10 mol L−1.
Authors and Affiliations
M. S. Attia, A. O. Yuossef, M. Diab, M. F. El-Shahat
Optimum Design of Shell and Tube Heat Exchanger Using Artificial Immune System Approach
This paper presents the economic optimization of shell and tube heat exchangers design approach through an artificial immune system algorithm for minimizing the cost. Since complex geometric parameters, with thermodynami...
A Facile One-pot Synthesis of New Pyrazolopyrimidines and Pyrazolo Pyridines Derivatives
A Simple Facile One-pot reaction, novel and efficient rout for the synthesis of substituted pyrazolo [3, 4-d] pyrimidines, and pyrazolo [3, 4-b] pyridines, results from reaction of substituted-5-amino-4-cyanopyrazoles wi...
Novel removal of Anthracene from oil-contaminated water by synthesized modified magnetic nano-particles
Novel magnetic nanoparticles (MNPs) modified with (3-mercaptopropyl)-trimethoxysilane (MPTMS), grafted with allyl glycidyl ether and coupled with beta naphthol, were prepared for removal of anthracene in aqueous solution...
Acid Attack on Reinforced Concrete Incorporated with Industrial Wastes
The study was conducted to evaluate the durable characteristics of Reinforced Concrete with silica fume and copper slag. The concrete mix design was done for M40 grade concrete with 7% silica fume as cement and 10 to 30%...
Metal Oxide Porous Coatings for Implantant Materials
The paper presents the results of study of synthesis of metal oxide coatings on porous materials used in implant surgery (stainless steel 12X18H9T, titanium alloy and high-purity niobium VT5). It is shown the prospects o...