Study on Synthesis and Characterization of Hexaquonickel(II) bis-p-toluenesulfonate
Journal Title: Asian Journal of Chemical Sciences - Year 2017, Vol 3, Issue 2
Abstract
Hexaquonickel (II) bis-p-toluenesulfonate [Ni(OTs)2•6H2O] was prepared from the reaction of p-toluenesulfonic acid (PTS) and nickel hydroxide [Ni(OH)2]. Energy disperse spectroscopy, thermal-analysis instrument, infrared spectrometer, and X-ray diffractometer were used to characterize the product of Ni(OTs)2•6H2O purified by recrystallization. The influence of equivalence ratio of reactants [NPTS/NNi(OH)2], reaction temperature and reaction time on the yield of products was investigated. The results show that when the value of NPTS/NNi(OH)2 is 1.1, reaction temperature is 353 K, and reaction time is 3 h, the yield of the product is 90.86%.
Authors and Affiliations
Wu Shutian, Zhu Qinyu, Guo Wenhui, Xiong Wanli, Tang Shiyi, Xue Weilan, Zeng Zuoxiang
Keywords
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- EP ID EP338844
- DOI 10.9734/AJOCS/2017/35519
- Views 110
- Downloads 0
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