Syntheses and Characterization of 1-D Titanium Glycolate microstructures: Effect of Dilution and Addition type on the Morphology of microstructures
Journal Title: International Journal of Engineering and Science Invention - Year 2017, Vol 6, Issue 11
Abstract
Titanium glycolate is synthesized by the reaction of titanium butoxide with monoethylene glycol. This is a quick and convenient method for the preparation of titanium glycolate; the glycol acts as both reactant as well as solvent in the reaction. None of earlier studies reported in prior arthave attempted a detailed investigation into factors influencing the transition of the multidimensional Ti glycolate structure to the one dimensional (1-D) Ti glycolate structure, though previous studies report the formation of titanium glycolates possessing different shape and size characteristics (i.e. micro-rods, whiskers, wires, and so forth) at varying syntheses conditions. This paper reports the transition of multi-dimensional to 1-D Ti glycolate structures (transition from micro-rods to nanowires) through a detailed investigation of key process parameters which direct the formation of a 1-D structure. The characterization of the as-prepared titanium glycolates has been conducted using various analytical techniques viz. Scanning electron microscopy (SEM), Thermo-gravimetric analyses (TGA, TGA-MS); Inductively Coupled Plasma – Optical Emission spectroscopy (ICP-OES), Fourier Transform Infrared spectroscopy (FT-IR) and Elemental analysis (CHNS).
Authors and Affiliations
Shilpa Shinde, Abha Dhomane, Mahesh Subramaniyam
Keywords
Related Articles
- EP ID EP403626
- DOI -
- Views 44
- Downloads 0
Extensive Security and Performance Analysis Shows the Proposed Schemes Are Provably Secure and Highly Efficient
In this paper, we utilize the public key based homomorphism authenticator and uniquely integrate it with random mask technique to achieve a privacy-preserving public auditing system for cloud data storage security while...
Influences of Solar Activities on Earthquakes during Different two Solar Cycles 22 and 23
The Sun as a primary source of radiant energy is an active object to Earth as it emits a large amount of radiation with a wide range of wavelengths, and energetic charged particles which have severe effects on the man-ma...
Physiochemical and Phytochemical Characteristics of LesserKnown Nigerian Black Melon (Ahu Agba) Seed Flour
The physiochemical and phytochemical properties of a lesser-known Nigerian black melon (ahu agba) seed flour was determine in this study. Foaming capacity, emulsion capacity, oil absorption, water absorption, and bulk de...
Present Status of Insecticides Use for The Cultivation of Brinjal in Kushtia Region, Bangladesh
This study has been carried out to assess the present status of insecticides use for the cultivation of brinjal in Kushtia region. A total number of 240 brinjal growers were randomly selected and interviewed by structure...
An Eco-System of SDR, SDN and Massive MIMO for 5G Networks
In this paper we are presenting the integration of state-of-the-art technologies like Software Defined Radio (SDR),Software defined Network, Network Function Virtualization and Massive Multiple Input Multiple Output (MIM...