Syntheses and Characterization of 1-D Titanium Glycolate microstructures: Effect of Dilution and Addition type on the Morphology of microstructures
Journal Title: International Journal of Engineering and Science Invention - Year 2017, Vol 6, Issue 11
Abstract
Titanium glycolate is synthesized by the reaction of titanium butoxide with monoethylene glycol. This is a quick and convenient method for the preparation of titanium glycolate; the glycol acts as both reactant as well as solvent in the reaction. None of earlier studies reported in prior arthave attempted a detailed investigation into factors influencing the transition of the multidimensional Ti glycolate structure to the one dimensional (1-D) Ti glycolate structure, though previous studies report the formation of titanium glycolates possessing different shape and size characteristics (i.e. micro-rods, whiskers, wires, and so forth) at varying syntheses conditions. This paper reports the transition of multi-dimensional to 1-D Ti glycolate structures (transition from micro-rods to nanowires) through a detailed investigation of key process parameters which direct the formation of a 1-D structure. The characterization of the as-prepared titanium glycolates has been conducted using various analytical techniques viz. Scanning electron microscopy (SEM), Thermo-gravimetric analyses (TGA, TGA-MS); Inductively Coupled Plasma – Optical Emission spectroscopy (ICP-OES), Fourier Transform Infrared spectroscopy (FT-IR) and Elemental analysis (CHNS).
Authors and Affiliations
Shilpa Shinde, Abha Dhomane, Mahesh Subramaniyam
Keywords
Related Articles
- EP ID EP403626
- DOI -
- Views 57
- Downloads 0
Productivity of a Residential Building
In recent treads a wide range of building materials are available for the construction of civil engineering structures. The total cost of materials may be up to 60% or more of the total cost incurred in construction proj...
Improved Particle Filter For Nor-Linear Noisy Observation Series
The particle filtering (PF) theory is a very method to denoise the non-linear disturbed signals. It could disposal signals with non-Gauss noise which can’t be done by Kalman filtering (KF). The theory is widely used in t...
A Modified Halpin-Tsai Model for Estimating the Modulus of Natural Fiber Reinforced Composites
The modulus of composites formed from three selected natural fiber sources (Empty Plantain Bunch Fiber, Empty Palm Bunch Fiber and Rattan Palm Fiber) - mercerized at optimum conditions - with two selected thermosetting r...
The Use οf Wireless Sensors Network for Supporting Human Daily Activities
This paper presents the comparative study of wireless sensors network, which are applied in a domestic environment, in the assembly production line of an industrial environment and in environmental applications. More spe...
Synthesis and Biological Evaluation of Chalcones as Potential Anti Fungal Agents
AseriesofchalconesweresynthesizedandelucidatedstructurallybyIRand1HNMRspectroscopies.The syntheticcompounds were then screened for antifungal activity using cup plate method against three fungal strains Aspergillus niger...