SYNTHESIS AND CHARACTERIZATION OF INTERPENETRATING POLYMER NETWORK OF POLY (METHYLHYDROSILOXANE) AND POLY (ACRYLONITRILE).
Journal Title: International Journal of Advanced Research (IJAR) - Year 2018, Vol 6, Issue 12
Abstract
Interpenetrating polymer network (IPN) based on poly (Methylhydrosiloxane) and poly (Acrylonitrile) have been synthesized using benzyl peroxide as initiator and divinyl benzene as crosslinker in toluene under an inert atmosphere of nitrogen. The scanning electron microscopy reveals dual phase morphology of the synthesized polymer network. The properties like percentage swelling, average molecular weight between crosslink?s (Mc), are the direct function of [copolymer] and initiator [benzoylperoxide] whereas inverse function of concentration of monomer (acrylonitrile) and crosslinker (divinyl benzene). A fluorescence spectrum of the material is observed in the visual range near 457 nm. FTIR spectrum confirmed the presence of PMHS and acrylonitrile and DVB in the synthesized IPN. The differential scanning calorimeter (DSC) curve showed glass transition temperature at 340oC. Thermogravimetric analysis (TGA) depicted thermal stability of IPN upto 400oC. The synthesized IPN is thermally stable upto 400oC.
Authors and Affiliations
Dayanand mishra, meet kamal.
Keywords
Related Articles
- EP ID EP448055
- DOI 10.21474/IJAR01/8257
- Views 79
- Downloads 0
DEVELOPMENT OF SUBJECT LEARNING DEVICES ASSESSMENT OF ECONOMIC LEARNING RESULTS USING CONTEXTUAL TEACHING AND LEARNING APPROACH IN STKIP PGRI SUMBAR.
The Contextual Teaching and Learning is one approach that can overcome learning problems in Learning Economic Learning Outcomes Assessment. Contextual Teaching and learning has several components that can be implemented...
IMPROVING MOTIVATION AND STUDENT LEARNING OUTCOME ON GEOMETRY TRANSFORMATIONSUBJECT WITH USING MODULES BASED ON GUIDED DISCOVERY.
Motivation and student learning outcomes depend on the learning strategy, learning media, and teaching materials used. Teaching materials used in the subject of Geometry transformation has not been able to increase motiv...
PATTERNS OF INTENTS, DECISIONS, AND TENDENCIES BASED ON BEHAVIORAL STYLES.
Human behavior is the expression of held values and beliefs. While it is correct to believe that behavior can adjust over time due to the shift in personality that?s being expressed, after a certain age, the personality...
SURGICAL MANAGEMENT OF CANINE ORAL TUMORS.
Five male dogs with age ranging from 5 -9 years, and different breeds viz., Labrador, St. Bernard, Spitz, GSD and Mongrel one each presented to the Department of Surgery and Radiology, CVSc, Rajendranagar, PVNR TVU with...
STABILITY STUDY OF POLYPHENOLS EXTRACTED FROM THE LEAF SHEATH OF RED SORGHUM (SORGHUM CAUDATUM) FROM BENIN.
L?extrait brut aqueux de la gaine foliaire du sorgho rouge est tr?s utilis? au B?nin et dans la sous-r?gion ouest-africaine ? des fins alimentaires et/ou pharmacologiques. Cependant, les conditions de son extraction-cons...