One-pot route to nitriles from aldehyde and hydroxylamine hydrochloride on silica-gel
Journal Title: Asian Journal of Green Chemistry - Year 2018, Vol 2, Issue 4
Abstract
A green and facile methodology for the synthesis of nitrile has been established from the corresponding aldehydes and hydroxylamine hydrochloride on silica-gel in hot condition. The protocol is equally effective for aliphatic as well as aromatic aldehydes, and has wide range of functional group tolerance. In addition, this methodology is solvent-free, inexpensive, environmental friendly and involves simple work-up process.
Authors and Affiliations
Rakesh Ranjan Chakraborty, Pranab Ghosh
Keywords
Related Articles
- EP ID EP468812
- DOI 10.22034/ajgc.2018.62809
- Views 75
- Downloads 0
Highly asymmetric aldol reaction of cyclohexanone and aromatic aldehydes catalyzed by bifunctional cyclohexane derived thiourea organocatalyst
Novel two L-proline analogues as thiourea organocatalysts were synthesised, first is the assembly of a structurally well-defined cyclohexane scaffold with a thiourea moieties and amine functionalities could constitute a...
Emblica officinalis leaf extract mediated synthesis of zinc oxide nanoparticles for antibacterial and photocatalytic activities
ZnO nanoparticles have been synthesized via a simple green method using plant extract without the use of any other chemicals. The synthesized ZnO nanoparticles were characterized by UV–vis diffuse reflectance spectroscop...
Synthesis of carbohydrazide and using it for green synthesis of oxazol and a substitute for hydrazine in the deoxygenation of water supply from boilers
Oxazole derivatives were prepared via multicomponent reaction of carbohydrazide, dialkyl acetylenedicarboxylate and ketone at room temperature under solvent-free conditions in good yields. One of the alternative materia...
Eco-friendly biosynthesis of silver nanoparticles using aqueous solution of Spartium junceum flower extract
Green synthesis of nanoparticles has received great attention from scientists due to their undeniable applications in all field of science. In this study, an eco-friendly and fast approach is reported for the preparation...
Identification and characterization of diterpenes from ethyl acetate fraction of stem barks of Boswellia papyrifera (del) hochst, sudanese medicinal plant
In this study, the diterpen compounds present in the ethyl acetate fraction of stem bark of Boswellia papyrifera grown in Sudan were investigated using gas chromatography-mass spectrometry (GC-MS), based upon interpretat...