Synthesis of Poly Azo Heterocyclic from Modification of Poly Methyl Acrylate
Journal Title: IOSR Journal of Pharmacy and Biological Sciences (IOSR-JPBS) - Year 2017, Vol 12, Issue 2
Abstract
In this study, the new polymers were synthesized from polymerization of methyl acrylate, then reacted with hydrazine hydrate in presence of ethanol to prepared polymer (b) . This polymer was reacted with KOH , carbon disulfide (CS2), 10% hydrochloric acid and ethanol as solvent to product polymer (c), then reacted with hydrazine hydrate to prepared polymer (d) which form diazonium salt by reacted with NaNO2 and conc. HCl at 0C0 to form polymer (e) . Acetylacetone was added to polymer (e) in basic media to product azo hetero polymer , then reacted with hydrazine and their derivatives to form new hetero ring on azo hetero polymer .All prepared polymers were identified by physical properties ,FT-IR and some of them 1H-NMR .
Authors and Affiliations
Entesar O. AlTamimi, Sura S. AlKaissi*, Aymen A . Dagher*
Keywords
Related Articles
- EP ID EP388369
- DOI 10.9790/3008-1202010612
- Views 76
- Downloads 0
Combined Ethanol Leaf Extract of Sour Sop (Anonna Muricata) and Jackfruit (Artocarpus Heterophyllus) Leaves Amelioratesstreptozotocin Induced Type 2 Diabetes Mellitus In Wistar Albino Rats
Type 2 diabetes results from the inability of islet cells of the pancreas to produce insulin which regulates blood sugar. A lot of natural products have proven effective in the treatment of diabetes mellitus due to their...
Male Aphrodisic Screening of Plants Mucuna Prurita, Mesua Ferrea, Punica Granatum on Rats
India has a rich culture of medicinal herbs and spices, including Ayurvedic, Unani, Siddha and other traditional medicines but only very few have been studied chemically and pharmacologically for their potential medicina...
Determination of Minimum Inhibitory Concentration for Chitosan Extracted from Metapeuous monoceros Against Gram Positive Bacteria, Gram Negative Bacteria and Fungi.
Chitin is a polysaccharide of animal origin found abundantly in nature and characterized by a fibrous structure. It forms the basis of the main constituent of the outer skeleton of insects and crustaceans like shrimp, cr...
Serum Thyroid Hormone Levels in Sudanese Patients with Liver Cirrhosis
Background: There are clinical and laboratory associations between thyroid and liver diseases. Patients with chronic liver disease such as cirrhosis may have thyroiditis, hyperthyroidism, or hypothyroidism, because thyro...
Lipases, Definition, and their Application
Esterase and lipase have been consisted of α/β hydroxylase super family that characterized primarily by their α/β hydroxylase fold (common fold), which is in the center, pre-dominantly parallel β-sheet and flanked via th...