The Synthesis and Characterization of Calcium Carbonate in the Presence of Polyelectrolyte and Experimental Design

Abstract

In this study, calcium carbonate (CaCO3) was synthesized by means of ultrasonic irradiation process in the presence of the water-soluble polyelectrolyte Poly(Vinyl Sulfonic Acid) (PVS). Synthesized CaCO3 crystals were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Particle size distribution analysis and thermal analysis (TGA-DTA). The effects of the amplitude of sonicator, polymer concentration and the application time of ultrasound on the obtained CaCO3 with respect to particle size of final product was investigated by applying the 2k Factorial Design. The experimental design was studied at two levels. All the selected process parameters were found to be very effective on the particle size of calcium carbonate obtained in the presence of PVS. The order of factor strength on particle size was polymer concentration > the application time of ultrasound > the amplitude of sonicator.

Authors and Affiliations

Semra KIRBOĞA

Keywords

Related Articles

Design and Numerical Analysis of a Double-Tube Magnetorheological Shock Absorber for Vehicle Seat Suspension Systems

In scissors-type suspension mechanisms of the driver's seats of vehicles such as tractors, trucks and buses, conventional double-tube shock absorbers are often used as dampers due to the length of the course. The damping...

BRIQUETTING OF AFŞİN-ELBİSTAN LIGNITE USING BIOMASS AND BINDER ADDITIVES

In this study, a lignite sample from Afşin-Elbistan area of Turkey was briquetted using hazelnut shell, sunflower shell and prina as additives. The lignite and biomass samples were first briquetted separately without ble...

Artificial Neural Network Based Early Warning System For Aydin Province Towards Air Factors Which Primarily Affect Human Health

Temperature, air quality index and ultraviolet index, which are basic air parameters, affect human health significantly. It is important to inform people about the precautions to be taken for these factors affecting huma...

The Effect of Explosıve Ratıo on Interface Formatıon in Explosıon Weldıng of Non Alloyed and Austenıtıc Steel Plates

In this study, weldability of austenitic stainless steel sheet to DKP sheet metals by explosive welding and the effect of explosive ratio (Elbar 5) on the joint interface have been investigated experimentally. Experiment...

Design of a Semi-Autonomous Electric Wheelchair Controlled by Head Movements

In this study, the design and development of a semi-autonomous electric wheelchair which is controlled by head movements is explained. For the system to function at the desired level, various algorithms are specially ada...

Download PDF file
  • EP ID EP485567
  • DOI 10.29109/http-gujsc-gazi-edu-tr.369221
  • Views 78
  • Downloads 0

How To Cite

Semra KIRBOĞA (2017). The Synthesis and Characterization of Calcium Carbonate in the Presence of Polyelectrolyte and Experimental Design. Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji, 5(4), 59-70. https://europub.co.uk/articles/-A-485567